Lithium Hydroxide → 5-Methoxyquinoline-3-carboxylic acid

HRID 880961노트

반응식

HRID 880961 반응식
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:4]=1[CH:5]=[C:6]([C:13]([O:15]C)=[O:14])[CH:7]=[N:8]2.[OH-].[Li+]>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][CH:10]=[C:9]2[C:4]=1[CH:5]=[C:6]([C:13]([OH:15])=[O:14])[CH:7]=[N:8]2

참가 물질

3

반응물 2

HCID 3939Lithium HydroxideHCID 57440609HCID 57440609, 화합물

생성물 1

HCID 231597415-Methoxyquinoline-3-carboxylic acid

실험 절차

Methyl 5-methoxyquinoline-3-carboxylate (Organic and Biomolecular Chemistry, 7(12), 2612-2618; 2009) was saponified using aqueous lithium hydroxide. +ESI (M+H) 203.9; 1H NMR (400 MHz, DMSO-d6, δ): 9.30 (d, 1H), 9.03 (d, 1H), 7.84-7.80 (m, 1H), 7.66 (d, 1H), 7.15 (d, 1H), 4.04 (s, 3H).

출처 및 근거

ORD 기록
ord-352df0b3db044c10a6bc87cb9eebe5ff
출처 데이터셋
uspto-grants-2015_03
특허 번호
US08993586B2

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