Stannous Chloride → 3-(2-Amino-4-methyl-phenylsulfanyl)-phenol

HRID 883885노트

반응식

HRID 883885 반응식
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-])=O)[CH:3]=1.Cl[Sn]Cl>>[NH2:16][C:4]1[CH:3]=[C:2]([CH3:1])[CH:7]=[CH:6][C:5]=1[S:8][C:9]1[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=1

참가 물질

3

반응물 2

HCID 24479Stannous ChlorideHCID 602047953-(4-Methyl-2-nitro-phenylsulfanyl)-phenol

생성물 1

HCID 574699063-(2-Amino-4-methyl-phenylsulfanyl)-phenol

실험 절차

The product from Example 25a was reduced with SnCl2 following the procedure from Example 7f giving the title compound.

출처 및 근거

ORD 기록
ord-7ce05199c00641d89ba892125978f031
출처 데이터셋
uspto-grants-2012_08
특허 번호
US08236950B2

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