Ethionamide → HCID 22249370, 화합물
반응식
[CH3:1][CH2:2][C:3]1[CH:8]=[C:7]([C:9]([NH2:11])=S)[CH:6]=[CH:5][N:4]=1>CO.[Ni]>[CH2:2]([C:3]1[CH:8]=[C:7]([CH2:9][NH2:11])[CH:6]=[CH:5][N:4]=1)[CH3:1]참가 물질
4
실험 절차
To a solution of 2-ethyl-4-thiopyridylamide (10 g) in MeOH (250 ml) was added Raney 2800 Nickel (5 g, Aldrich) in one portion. The mixture was stirred at RT for 2 days then at 60° C. for 16 h. The mixture was filtered, concentrated to provide the desired compound.
후처리
- waitat 60° C. for 16 h
- filtrationThe mixture was filtered
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-32dabe87641849c5ac32f6c75c2c0847
- 출처 데이터셋
- uspto-grants-2012_08
- 특허 번호
- US08247430B2
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