Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Salicylic acid, hydrazide → HCID 178513059, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Salicylic acid, hydrazide | HCID 13637 | — |
| 반응물 | Methyl 2,2,2-trichloroacetimidate | HCID 100479 | — |
| 생성물 | HCID 178513059 | HCID 178513059 | 100% |
반응 단계
A mixture of 3.8 g (0.025 mole) salicoylhydrazine and 10 ml (14.3 g, 0.08 mole) methyl 2,2,2-trichloroacetimidate was stirred 16 hours at room temperature. The solid that formed was washed with petroleum ether and dried to give 7.5 g (100% Yield; mp 168°-169° C.). The structure was confirmed via infrared and elemental analysis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04282169 |
| 출처 데이터셋 | uspto-grants-1981_08 |
| ORD ID | ord-88e76842bc034e489c23448c2f0c5573 |
| 출처 메모 | uspto-grants-1981_08 |