反应详情

A mixture of 3.8 g (0.025 mole) salicoylhydrazine and 10 ml (14.3 g, 0.08 mole) methyl 2,2,2-trichloroacetimidate was stirred 16 hours at room temperature. The solid that formed was washed with petroleum ether and dried to give 7.5 g (100% Yield; mp 168°-169° C.). The structure was confirmed via infrared and elemental analysis.

1. customThe solid that formed
2. washwas washed with petroleum ether
3. customdried
4. customto give 7.5 g (100% Yield; mp 168°-169° C.)