홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Sodium Hydroxide → 4-(3-(2,6-Dimethylbenzyloxy)phenyl)-3-butenoic acid

HRID 895757
노트
인쇄 미리보기

반응식

HRID 895757 반응식
[CH3:1][C:2]1[CH:23]=[CH:22][CH:21]=[C:20]([CH3:24])[C:3]=1[CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH:12]=[CH:13][CH2:14][C:15]([O:17]CC)=[O:16])[CH:9]=[CH:10][CH:11]=1.[OH-].[Na+]>C(O)C>[CH3:24][C:20]1[CH:21]=[CH:22][CH:23]=[C:2]([CH3:1])[C:3]=1[CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH:12]=[CH:13][CH2:14][C:15]([OH:17])=[O:16])[CH:9]=[CH:10][CH:11]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 67274119Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate

생성물 1

HCID 672736064-(3-(2,6-Dimethylbenzyloxy)phenyl)-3-butenoic acid

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate (Step F) in abs ethanol at low temp, add aqueous sodium hydroxide, after an hour, concentrate and purify by flash chromatography on silica gel column (chloroform:methanol 95:5 spiked with acetic acid).

후처리

  1. waitafter an hour
  2. concentrationconcentrate
  3. custompurify by flash chromatography on silica gel column (chloroform:methanol 95:5 spiked with acetic acid)

출처 및 근거

ORD 기록
ord-d9d6bbb4830348a8aadc2c263e1b8581
출처 데이터셋
uspto-grants-2005_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06916848B2

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트