Ethanol → 2-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine

HRID 903321노트

반응식

HRID 903321 반응식
[Na].ClC1N=NN=C(Cl)C=1.[Cl:10][C:11]1[N:16]=[C:15](Cl)[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1.[CH2:21]([OH:23])[CH3:22]>>[Cl:10][C:11]1[N:16]=[C:15]([O:23][CH2:21][CH3:22])[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1

참가 물질

5

반응물 4

HCID 702Ethanol2회HCID 169852,4-Dichloro-6-(dimethylamino)-1,3,5-triazineHCID 5360545SodiumHCID 18348308HCID 18348308, 화합물

생성물 1

HCID 233381422-Chloro-4-ethoxy-6-dimethylamino-1,3,5-triazine

실험 절차

A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C.) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.

후처리

  1. additionthe addition the solution
  2. customthe product collected
  3. customdried
  4. customcrystallised from petroleum as needles (2.5 g.)

출처 및 근거

ORD 기록
ord-66b37f85eaa14fb1b300dbb4ab41495e
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04226990

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