Veratraldehyde → HCID 54360198, 화합물

HRID 903427노트

반응식

HRID 903427 반응식
[CH3:1][C:2]([C:4]1([CH2:7][CH3:8])[CH2:6][CH2:5]1)=[O:3].[CH:9](=O)[C:10]1[CH:19]=[CH:18][C:15]([O:16][CH3:17])=[C:12]([O:13][CH3:14])[CH:11]=1>>[CH2:7]([C:4]1([C:2]([CH:1]=[CH:9][C:10]2[CH:19]=[CH:18][C:15]([O:16][CH3:17])=[C:12]([O:13][CH3:14])[CH:11]=2)=[O:3])[CH2:6][CH2:5]1)[CH3:8]

참가 물질

3

반응물 2

HCID 8419VeratraldehydeHCID 142008571-(1-Ethylcyclopropyl)ethan-1-one

생성물 1

HCID 54360198HCID 54360198, 화합물

실험 절차

2-(3,4-Dimethoxyphenyl)vinyl 1-ethylcyclopropyl ketone [III; Ar is 3,4-(CH3O)2C6H3, R is C2H5 ] was prepared from 22.4 g. of 1-ethylcyclopropyl methyl ketone and 33.2 g. of veratraldehyde according to the procedure described above in Preparation A1, affording 20.3 g., b.p. 156°-158° C. (0.02 mm.).

후처리

  1. customaffording 20.3 g

출처 및 근거

ORD 기록
ord-9497bb6bdea84602b1d1e3da5a335c89
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04227015

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