Acetic Anhydride → alpha-(2-Acetoxy-5-sulfophenylazo)acetoacetanilide

HRID 903524노트

반응식

HRID 903524 반응식
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([OH:11])(=[O:10])=[O:9])=[CH:4][C:3]=1[N:12]=[N:13][CH:14]([C:24]([CH3:26])=[O:25])[C:15]([NH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[O:16].[C:27](OC(=O)C)(=[O:29])[CH3:28]>N1C=CC=CC=1>[C:27]([O:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([OH:11])(=[O:10])=[O:9])=[CH:4][C:3]=1[N:12]=[N:13][CH:14]([C:24]([CH3:26])=[O:25])[C:15]([NH:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)=[O:16])(=[O:29])[CH3:28]

참가 물질

4

반응물 2

HCID 7918Acetic AnhydrideHCID 135839437alpha-(2-Hydroxy-5-sulfophenylazo)acetoacetanilide

생성물 1

HCID 23336111alpha-(2-Acetoxy-5-sulfophenylazo)acetoacetanilide

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

α-(2-Hydroxy-5-sulfophenylazo)acetoacetanilide (40 g) was dissolved in boiling pyridine (750 ml) and acetic anhydride (100 ml) added. Some material precipitated while the reaction mixture was hot. After being cooled, the product was filtered off and dried.

후처리

  1. additionadded
  2. customSome material precipitated while the reaction mixture
  3. temperatureAfter being cooled
  4. filtrationthe product was filtered off
  5. customdried

출처 및 근거

ORD 기록
ord-3f46446a15a84148b7645cc88a2f6abd
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04228073

반응 노트

불러오는 중…