Diazomethane → HCID 20528716, 화합물

HRID 903870노트

반응식

HRID 903870 반응식
[C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])([OH:3])=[O:2].[N+](=[CH2:17])=[N-]>CCOCC>[CH3:17][O:2][C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])=[O:3]

참가 물질

4

반응물 2

HCID 9550DiazomethaneHCID 205447191,3-dioxo-2,3-dihydro-1H-isoindole-4-carboxylic acid

생성물 1

HCID 20528716HCID 20528716, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매2회

실험 절차

To a suspension of 3-carboxyphthalimide (10 g) in ether (50 ml), a solution of diazomethane in ether was added slowly until a faint yellow colouration persisted. Excess of diazomethane was destroyed with acetic acid and the reaction mixture was evaporated to yield the desired compound.

후처리

  1. customExcess of diazomethane was destroyed with acetic acid
  2. customthe reaction mixture was evaporated

출처 및 근거

ORD 기록
ord-d285e306ed5e42b19ca3f0039a71a8b7
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04229443

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