Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Cyanide → 12-Hydroxydodecanenitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Cyanide | HCID 8929 | — |
| 반응물 | 11-Bromo-1-undecanol | HCID 74163 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 12-Hydroxydodecanenitrile | HCID 10330348 | — |
반응 단계
A solution 4.6 g. of 11-bromoundecanol and 1.6 g. of sodium cyanide in 40 ml. of dimethylformamide is heated at 80° C. for 18 hours, cooled, and poured into ice-water. The mixture is extracted with methylene chloride and the extract is dried over anhydrous magnesium sulfate. Evaporation of the solution affords 12-hydroxydodecanonitrile as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04230628 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-af4d2d2762314fcc986794205f24620b |
| 출처 메모 | uspto-grants-1980_10 |