Butyl Formate → Dibutyl Oxalate

HRID 904933

반응식

HRID 904933 반응식
[CH:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])=[O:2]>C(O)CCC>[C:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])(=[O:2])[C:1]([O:3][CH2:4][CH2:5][CH2:6][CH3:7])=[O:2]

참가 물질

3

반응물 1

HCID 11614Butyl Formate

생성물 1

HCID 16306Dibutyl Oxalate

시약·촉매·용매 1

HCID 2631-Butanol용매

실험 절차

Experiment was run in the same manner as in Example 4 except that the catalyst was replaced by 1.0 wt.% palladium-on-silicon-carbide. As the result, it was found that n-butyl formate was produced in a space time yield of 202 g./l.-catalyst.hr and small amounts of di-n-butyl oxalate and n-butanol were by-produced.

후처리

  1. customwas produced in a space time yield of 202 g

출처 및 근거

ORD 기록
ord-57f0fcd15f7c4a6a815b1edb34f42b7d
출처 데이터셋
uspto-grants-1983_12
특허 번호
US04420633

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