Benzyl Chloride → 3-Benzyl-2,2,5,5-tetramethyl-4-oxo-imidazolidine

HRID 918359노트

반응식

HRID 918359 반응식
[CH3:1][C:2]1([CH3:10])[NH:6][C:5](=[O:7])[C:4]([CH3:9])([CH3:8])[NH:3]1.[CH2:11](Cl)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([N:6]1[C:5](=[O:7])[C:4]([CH3:9])([CH3:8])[NH:3][C:2]1([CH3:10])[CH3:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

3

반응물 2

HCID 7503Benzyl ChlorideHCID 98127982,2,5,5-Tetramethyl-4-imidazolidinone

생성물 1

HCID 215207973-Benzyl-2,2,5,5-tetramethyl-4-oxo-imidazolidine

실험 절차

If, instead of 7,14-diaza-15-oxo-dispiro[5.1.5.2]pentadecane, 2,2,5,5-tetramethyl-4-oxo-imidazolidine is used, and this alkylated with benzyl chloride as described in Example 1, then 3-benzyl-2,2,5,5-tetramethyl-4-oxo-imidazolidine (VII), M.P. 210°C, is obtained.

출처 및 근거

ORD 기록
ord-0b39d41fc52a4d9daba8b65d702fd22b
출처 데이터셋
uspto-grants-1976_07
특허 번호
US03971757

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