참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| 반응물 | Ethyl 2-ethoxy-2-iminoacetate | HCID 10920638 | — |
| 생성물 | HCID 58081363 | HCID 58081363 | — |
반응 단계
Ethyl-2-ethoxy-2-iminoacetate (1.318 g, 9.08 mmol) and phenyl acetic acid hydrazide (1.364 g, 9.08 mmol) were mixed together in ethanol (20 ml) and stirred at 80° C. for 1 h. Ethanol was evaporated. The residue was dissolved in n-butanol (20 ml). The reaction mixture was stirred at 150° C. for 20 h, then solvents were evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09290485B2 |
|---|
| 출처 데이터셋 | uspto-grants-2016_03 |
|---|
| ORD ID | ord-12d0f595110f482ea4f4751a12afcd85 |
|---|
| 출처 메모 | uspto-grants-2016_03 |
|---|
