Bromoacetyl bromide → 5-(2-Bromoacetyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

반응식

[O:1]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[NH:5][CH2:4][CH2:3][CH2:2]1.[Br:12][CH2:13][C:14](Br)=[O:15]>>[Br:12][CH2:13][C:14]([N:5]1[C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:1][CH2:2][CH2:3][CH2:4]1)=[O:15]

참가 물질

반응물 2

HCID 61147Bromoacetyl bromide

HCID 5777522,3,4,5-Tetrahydro-1,5-benzoxazepine

생성물 1

HCID 196942555-(2-Bromoacetyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

실험 절차

2,3,4,5-tetrahydro-1,5-benzoxazepine [E. K. Orlova et al.; Kim. Geterotsikl. Soedin.,9, 1296 (1975): Chem. abstra., 84, 59411] and bromoacetyl bromide were used to produce the above compound in the same way as Reference Example 8.

후처리

customto produce the above compound in the same way as Reference Example 8

출처 및 근거

ORD 기록: ord-63a70aa1c69f4c69985323de9986a8eb
출처 데이터셋: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05723475

반응 노트

불러오는 중…