Adamantanone → N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide
반응식
[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[C:2]1=O)[CH2:8]2.[C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])(=[O:15])[NH:13][NH2:14]>CCCCCC>[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[C:2]1=[N:14][NH:13][C:12]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])=[O:15])[CH2:8]2참가 물질
4
실험 절차
A hexane solution containing 2-adamantanone (2 g) and tert-butyl carbazate (1.76) was heated to reflux for 3 hours. When the solution cooled, the title compound crystallized and was filtered (3.28 g). M. p. 175-177°.
후처리
- temperaturewas heated
- temperatureto reflux for 3 hours
- temperatureWhen the solution cooled
- customthe title compound crystallized
- filtrationwas filtered (3.28 g)
출처 및 근거
- ORD 기록
- ord-704dd1d4bb5545e08cbb6cdc82f57b0e
- 출처 데이터셋
- uspto-grants-1998_06
- 특허 번호
- US05760059
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