Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibromomethane → 4-Ethenylphenyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibromomethane | HCID 3024 | — |
| 반응물 | Benzaldehyde, 4-(acetyloxy)- | HCID 70144 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-Ethenylphenyl acetate | HCID 75821 | — |
반응 단계
Then a mixture obtained by mixing 32.8 g of p-acetoxybenzaldehyde (PABA) (0.2 mol) and 52.15 g of dibromomethane (0.3 mol) in 85 g of anhydrous DMF was dropping for 1 hour keeping the internal temperature at 50° C. Then agitation was continued for 40 minutes under the same temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05763560 |
| 출처 데이터셋 | uspto-grants-1998_06 |
| ORD ID | ord-f5345871b7384f1f9277df1f844feb36 |
| 출처 메모 | uspto-grants-1998_06 |