HRID963592
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Then a mixture obtained by mixing 32.8 g of p-acetoxybenzaldehyde (PABA) (0.2 mol) and 52.15 g of dibromomethane (0.3 mol) in 85 g of anhydrous DMF was dropping for 1 hour keeping the internal temperature at 50° C. Then agitation was continued for 40 minutes under the same temperature.
WORKUP
后处理
- customThen a mixture obtained
- customat 50° C
- waitThen agitation was continued for 40 minutes under the same temperature