HRID963592

反应详情

EQUATION

反应方程式

HRID 963592 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Then a mixture obtained by mixing 32.8 g of p-acetoxybenzaldehyde (PABA) (0.2 mol) and 52.15 g of dibromomethane (0.3 mol) in 85 g of anhydrous DMF was dropping for 1 hour keeping the internal temperature at 50° C. Then agitation was continued for 40 minutes under the same temperature.

WORKUP

后处理

  1. customThen a mixture obtained
  2. customat 50° C
  3. waitThen agitation was continued for 40 minutes under the same temperature