Sulfuric Acid → Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

HRID 963600노트

반응식

HRID 963600 반응식
COC(C1SC=CC=1S(NCC1C=CC2OCOC=2C=1)(=O)=O)=O.S(=O)(=O)(O)O.[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31].[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:45])([CH3:44])[CH3:43])(=[O:38])[CH:36]=[CH2:37].Br([O-])(=O)=O.[Na+].[Na+].[Na+].[Na+].[Na+].C(N(CC([O-])=O)CC([O-])=O)CN(CC([O-])=O)CC([O-])=O>O>[Cl-:34].[C:35]([O:39][CH2:40][CH2:41][N+:42]([CH3:44])([CH3:43])[CH3:45])(=[O:38])[CH:36]=[CH2:37].[C:29]([NH2:33])(=[O:32])[CH:30]=[CH2:31]

참가 물질

8

반응물 6

HCID 1118Sulfuric AcidHCID 6144Edetate SodiumHCID 6579AcrylamideHCID 162071Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1)HCID 3476271Methyl 3-(1,3-benzodioxol-5-ylmethylsulfamoyl)thiophene-2-carboxylateHCID 23668195Sodium Bromate

생성물 1

HCID 155211Prop-2-enamide;trimethyl(2-prop-2-enoyloxyethyl)azanium;chloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

An organic solution is prepared by combining a low odor paraffin oil (208.4 g), polyoxyethylene sorbitan monooleate (9.0 g) and polyoxyethylene sorbitan trioleate (32.6 g) in a reactor with stirring. To this solution is added an aqueous solution, adjusted to pH =3.5 with sulfuric acid, containing acrylamide (24.0 g), acryloxyethyltrimethyl ammonium chloride (80.2 g), sodium bromate (0.01 g), ethylenediaminetetraacetic acid tetra sodium salt (0.21 g), and water (145.58 g).

후처리

  1. customAn organic solution is prepared
  2. additionTo this solution is added an aqueous solution

출처 및 근거

ORD 기록
ord-69d9a655d6d3497e8bf69b25d6566d6a
출처 데이터셋
uspto-grants-1998_06
특허 번호
US05763523

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