Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Mesityl-3-nitropyridine → 2-Mesityl-3-pyridinamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Mesityl-3-nitropyridine | HCID 22249491 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | HCID 178418361 | HCID 178418361 | — |
| 생성물 | 2-Mesityl-3-pyridinamine | HCID 16741426 | 106.5% |
반응 단계
Palladium-carbon (10%, 0.6 g) was added to a solution of 2-mesityl-3-nitropyridine (5.99 g, 23 mmol) in ethanol (120 mL), followed by stirring for one day in hydrogen atmospher. The mixture was filtered through Celite and evaporated, to give the title compound (5.2 g) as white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06951865B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-c73ee1167547434ca4212285a5e42e77 |
| 출처 메모 | uspto-grants-2005_10 |