Methyl Isocyanate → N-Methyl-N'-[2-(3-pyridazinylmethylamino)ethyl]urea

HRID 972600노트

반응식

HRID 972600 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][NH:8][CH2:9][CH2:10][NH2:11])[N:2]=1.[CH3:12][N:13]=[C:14]=[O:15]>>[CH3:12][NH:13][C:14]([NH:11][CH2:10][CH2:9][NH:8][CH2:7][C:3]1[N:2]=[N:1][CH:6]=[CH:5][CH:4]=1)=[O:15]

참가 물질

3

반응물 2

HCID 12228Methyl IsocyanateHCID 21698444N-(3-pyridazinylmethyl)ethylenediamine

생성물 1

HCID 20557601N-Methyl-N'-[2-(3-pyridazinylmethylamino)ethyl]urea

실험 절차

Reacting N-(3-pyridazinylmethyl)ethylenediamine with methyl isocyanate by the procedure of Example 24, then concentrating and separating the residue by column chromatography gives the title compound.

후처리

  1. concentrationconcentrating
  2. customseparating the residue by column chromatography

출처 및 근거

ORD 기록
ord-a7d68d38d4b24272bfed6d6a07ca5510
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04053473

반응 노트

불러오는 중…