Benzylamine → N-benzyladamantane-1-carboxamide

HRID 972645

반응식

HRID 972645 반응식
[C:1]12([C:11](Cl)=[O:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH2:14]([NH2:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>C(OCC)C>[CH2:14]([NH:21][C:11]([C:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2)=[O:12])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

4

반응물 2

HCID 7504BenzylamineHCID 989151-Adamantanecarbonyl chloride

생성물 1

HCID 3826889N-benzyladamantane-1-carboxamide

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

Dissolve 2.0 g. of (10 mmoles) of 1-adamantane carboxylic acid chloride in 20 ml. of ethyl ether and add to 3.0 ml. (28.0 mmoles) of benzylamine and repeat the process of Example 11 to obtain the product of this example, m.p. 170°-172° C.

후처리

  1. dissolutionDissolve 2.0 g
  2. customto obtain the product of this example, m.p. 170°-172° C.

출처 및 근거

ORD 기록
ord-d6c8a2c31fbc49df83019c19b0fe4783
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04053509

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