Triethylamine → HCID 3120174, 화합물

HRID 972656노트

반응식

HRID 972656 반응식
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH2:8])=[CH:5][CH:4]=1.[C:11]12([C:21](Cl)=[O:22])[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2.C(N(CC)CC)C>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:8][C:21]([C:11]23[CH2:20][CH:15]4[CH2:14][CH:13]([CH2:19][CH:17]([CH2:16]4)[CH2:18]2)[CH2:12]3)=[O:22])=[CH:5][CH:4]=1

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 754524-MethoxybenzylamineHCID 989151-Adamantanecarbonyl chloride

생성물 1

HCID 3120174HCID 3120174, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

Subject 4.0 g. (29.0 mmoles) of p-methoxy-benzylamine, 5.7 g. (29.0 mmoles) of adamantane carboxylic acid chloride and 10 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from chloroform to obtain the product of this Example, m.p. 91°-94° C.

후처리

  1. customCrystallize the residue
  2. customobtained

출처 및 근거

ORD 기록
ord-2ca0e7739857428da143a5aff21e03d9
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04053509

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