Methanethiol → HCID 54522754, 화합물

HRID 973076노트

반응식

HRID 973076 반응식
[CH3:1][S:2][C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([N+:11]([O-])=O)[C:4]=1[C:5]#[N:6].[N+](C1C=CC=C([N+]([O-])=O)C=1C#N)([O-])=[O:15].CS>[Ni]>[NH2:11][C:7]1[CH:8]=[CH:9][CH:10]=[C:3]([S:2][CH3:1])[C:4]=1[C:5]([NH2:6])=[O:15]

참가 물질

5

반응물 3

HCID 878MethanethiolHCID 520718DinitrobenzonitrileHCID 12715768HCID 12715768, 화합물

생성물 1

HCID 54522754HCID 54522754, 화합물

시약·촉매·용매 1

HCID 935Nickel촉매

실험 절차

2-Amino-6-(methylthio) benzamide is prepared by Raney nickel reduction of 2-(methylthio)-6-nitrobenzonitrile which is prepared from 2,6-dinitrobenzonitrile and methylmercaptan following the procedure set forth in Example 75.

출처 및 근거

ORD 기록
ord-eb736dd129114ef4b524c428e6b57018
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04054666

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