Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 2-Amino-4-chlorobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 2,4-Dichlorobenzamide | HCID 75556 | — |
| 생성물 | 2-Amino-4-chlorobenzamide | HCID 12374837 | — |
반응 단계
190 g of 2,4-dichlorobenzamide was dissolved in 1.5 liters of aqueous ammonia, and to the resulting solution was added 100 g of cuprous chloride. The mixture was reacted at 80° C. for 15 hours in an autoclave, and then neutralized. The crystals deposited were collected by filtration. Yield: 122 g (71.5%)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05066577 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-70f469c15fe2496a9d058d1f1845b271 |
| 출처 메모 | uspto-grants-1991_11 |