Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole → 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-(3-Hydroxy-1-but-1-enyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 54086563 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 5-(3-Hydroxy-1-butyl)-3-(N-methyl-4-piperidyl)-1H-indole | HCID 19970945 | — |
반응 단계
Obtained from the title compound of Example 42 by a procedure similar to that described in Example 2, but using 10% palladium on charcoal as catalyst, as a foam. Rf 0.50 (SS 4). C,73.39; H,8.77; N,9.06. C18H26N2O; 0.125 CH2Cl2 requires C,73.28; H,8.91; N,9.43%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05607960 |
| 출처 데이터셋 | uspto-grants-1997_03 |
| ORD ID | ord-631587a7f2de4c9a86ff6b175d215833 |
| 출처 메모 | uspto-grants-1997_03 |