Hydrochloric Acid → HCID 86750549, 화합물

HRID 976012노트

반응식

HRID 976012 반응식
C[O:2][C:3](=[O:16])[C@@H:4]([NH2:15])[CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([O:12]C)=[O:11].[ClH:17]>>[ClH:17].[ClH:17].[NH2:15][C@@H:4]([CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([OH:12])=[O:11])[C:3]([OH:16])=[O:2]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 71474603(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester

생성물 1

HCID 86750549HCID 86750549, 화합물

실험 절차

(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester (1.65 g, 7.17 mmol) was heated under reflux with 6H HCl (10 ml, 60 mmol) for 2 hours. The solvent was then evaporated, the residue was dissolved in water (10 ml) and ethanol was added (100 ml). The white crystals were filtered off and dried in vacuum at 40° C.

후처리

  1. customThe solvent was then evaporated
  2. dissolutionthe residue was dissolved in water (10 ml)
  3. additionethanol was added (100 ml)
  4. filtrationThe white crystals were filtered off
  5. customdried in vacuum at 40° C.

출처 및 근거

ORD 기록
ord-e3de0dc4f3034c94952d772f35754d99
출처 데이터셋
uspto-grants-1997_03
특허 번호
US05610141

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