Saccharin → 1,2,3,4-Tetrahydroquinoline

HRID 976089

반응식

HRID 976089 반응식
S1(C2C(=CC=CC=2)C(=O)[NH:4]1)(=O)=O.[CH3:13]/[C:14](/O)=[CH:15]/[C:16]([CH3:18])=O.[CH3:20]/[C:21](/O)=[CH:22]/[C:23](C)=O.C/C(/O)=C/C(C)=O.[Fe]>C(OCCCO)(=O)C(C)=C.C1C=C2C(C=C(C([O-])=O)C=C2)=CC=1.C1C=C2C(C=C(C([O-])=O)C=C2)=CC=1.[Co+2]>[NH:4]1[C:18]2[C:16](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH2:15][CH2:14][CH2:13]1

참가 물질

5

반응물 2

HCID 5143SaccharinHCID 11110968Iron (III) acetylacetonate

생성물 1

HCID 694601,2,3,4-Tetrahydroquinoline

시약·촉매·용매 2

HCID 14048876Cobaltous 2-naphthenic acid촉매HCID 176943-Hydroxypropyl methacrylate용매3회

실험 절차

An adhesive formulation prepared and tested as in Example 1 containing hydroxypropyl methacrylate (8.15 g), saccharin (0.5 g), 0.1% cobalt naphthenate in hydroxypropyl methacrylate (1 g), 0.1% iron (III) acetylacetonate in hydroxypropyl methacrylate (0.25 g) and 1,2,3,4 tetrahydroquinoline (0.5 g) gave bond strengths of 3.3N/mm2 after 24 hours following air activation for 5 minutes.

후처리

  1. customAn adhesive formulation prepared

출처 및 근거

ORD 기록
ord-d5751018a2b341268b560326d6ffc467
출처 데이터셋
uspto-grants-1997_03
특허 번호
US05610251

연결된 노트

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