Methyl iodide → HCID 19377717, 화합물

HRID 979924노트

반응식

HRID 979924 반응식
[CH3:1][O:2][CH:3]([O:10][CH3:11])[CH2:4][NH:5][C:6]([NH:8][CH3:9])=[S:7].[I:12][CH3:13]>CC(=O)C>[IH:12].[CH3:11][O:10][CH:3]([O:2][CH3:1])[CH2:4][NH:5][C:6]([S:7][CH3:13])=[N:8][CH3:9]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 14518105HCID 14518105, 화합물

생성물 1

HCID 19377717HCID 19377717, 화합물수율 99%

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of 7.1 parts of N-(2,2-dimethoxyethyl)-N'-methylthiourea, 8.5 parts of iodomethane and 80 parts of 2-propanone was stirred overnight. The reaction mixture was evaporated, yielding 12.8 parts (99%) of methyl N-(2,2-dimethoxyethyl)-N'-methylcarbamimidothioate monohydroiodide (191).

후처리

  1. customThe reaction mixture was evaporated

출처 및 근거

ORD 기록
ord-dd0e6e38489e45d6b7c35b911d8909ac
출처 데이터셋
uspto-grants-1987_01
특허 번호
US04634704

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