Water → HCID 6410643, 화합물

HRID 985938노트

반응식

HRID 985938 반응식
Cl[C:2]1[N:3]=[N:4][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][C:7]=1[CH3:8].[CH3:15][O:16][CH2:17][CH2:18][NH2:19].O>C(O)CCC>[CH3:15][O:16][CH2:17][CH2:18][NH:19][C:2]1[N:3]=[N:4][C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:6][C:7]=1[CH3:8]

참가 물질

5

반응물 3

HCID 962WaterHCID 80182-MethoxyethylamineHCID 1199993-Chloro-4-methyl-6-phenylpyridazine

생성물 1

HCID 6410643HCID 6410643, 화합물

시약·촉매·용매 1

HCID 2631-Butanol용매

실험 절차

A mixture of 7 g of 3-chloro 4-methyl 6-phenyl pyridazine and 7 g of 2-methoxy ethylamine in 50 ml of butanol is taken to reflux for 4 days. The hot solution is poured into 200 ml of water and extracted with ethyl acetate. The organic solution is dried over magnesium sulfate then evaporated to dryness.

후처리

  1. temperatureto reflux for 4 days
  2. extractionextracted with ethyl acetate
  3. dry with materialThe organic solution is dried over magnesium sulfate
  4. customthen evaporated to dryness

출처 및 근거

ORD 기록
ord-e602df8abd8e4825ae7ea9a34796eb20
출처 데이터셋
uspto-grants-1987_12
특허 번호
US04710499

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