Potassium Carbonate → HCID 19858315, 화합물

HRID 985962노트

반응식

HRID 985962 반응식
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

생성물 1

HCID 19858315HCID 19858315, 화합물

시약·촉매·용매 1

HCID 24813Phosphorus oxychloride촉매

실험 절차

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and concentrated to give the product as an oil.

후처리

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-c08d7a259d0748bf9a260847ae432013
출처 데이터셋
uspto-grants-1987_12
특허 번호
US04710504

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