Furfural → (2-Furan-2-yl-imidazo[1,2-a]pyridin-3-yl)-(6-isocyano-hexyl)-amine

HRID 988987

반응식

HRID 988987 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[N+:8]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][N+:16]#[C-:17])#[C-:9].[CH:18](=O)[C:19]1[O:23][CH:22]=[CH:21][CH:20]=1>Cl(O)(=O)(=O)=O>[O:23]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:18]1[N:1]=[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][N:3]2[C:9]=1[NH:8][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][N+:16]#[C-:17]

참가 물질

5

반응물 3

HCID 7362FurfuralHCID 104392-AminopyridineHCID 33911051,6-Diisocyanohexane

생성물 1

HCID 9861428(2-Furan-2-yl-imidazo[1,2-a]pyridin-3-yl)-(6-isocyano-hexyl)-amine

시약·촉매·용매 1

HCID 24247Perchloric Acid용매

실험 절차

Compound (2) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml 1,6-diisocyanohexane solution (0.2 M, MC), 0.500 ml furfural solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).

출처 및 근거

ORD 기록
ord-d96a5ab203914d9e9f40a7757e41c7e6
출처 데이터셋
uspto-grants-2003_10
특허 번호
US06638933B2

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