Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nonanone → 3-Nonanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nonanone | HCID 61235 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Nonanol | HCID 12216 | 96.3% |
반응 단계
20.5 g (144 mmol) of 3-nonanone are initially charged in 200 ml of methanol, 5.45 g (144 mmol) of sodium borohydride are added a little at a time at room temperature and the mixture is stirred overnight. The solvent is removed under reduced pressure and the mixture is then acidified and extracted with dichloromethane. The organic phase is dried over sodium sulphate. Removal of the solvent gives 20 g (96%) of a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06458796B1 |
| 출처 데이터셋 | uspto-grants-2002_10 |
| ORD ID | ord-f63b7042858a417da8139487ee5a4ea2 |
| 출처 메모 | uspto-grants-2002_10 |