HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 18796408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 1-Piperazinecarboxaldehyde | HCID 82191 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Product | HCID 18796408 | HCID 18796408 | — |
Reaction Steps
To a solution of 1.02 g of formylpiperazine in 90 ml of acetone was added 0.1 g of 5% palladium carbon and the mixture was stirred under hydrogen atmosphere for 60 hours. The catalyst was filtered off and distilled off under reduced pressure to afford 1.31 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046201 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-209bc8714224470088ebf261be393b5d |
| Source note | uspto-grants-2000_04 |