Hydrocarbostyril → HCID 21853079, compound

HRID 1003446Notes

Reaction equation

HRID 1003446 reaction equation
[NH:1]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][C:2]1=[O:3].F[B-](F)(F)F.[CH3:17][O+](C)C>>[CH3:17][O:3][C:2]1[CH2:4][CH2:5][C:6]2[C:11](=[CH:10][CH:9]=[CH:8][CH:7]=2)[N:1]=1

Participants

3

Reactant 2

HCID 64796HydrocarbostyrilHCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)

Product 1

HCID 21853079HCID 21853079, compound

Procedure

A sample of 3,4-dihydrocarbostyril (Apin Chemicals Ltd., 736 mg, 5.0 mmol) was reacted with trimethyloxonium tetrafluoroborate (924 mg, 6.2 mmol) by the method of EXAMPLE 26 to yield, after chromatography, 130 mg (16%) of the title material.

Workup

  1. customto yield

Sources & evidence

ORD record
ord-1083eb388b84432d8ba740db2fa33182
Source dataset
uspto-grants-2000_04
Patent number
US06046211

Reaction notes

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