HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(tert-Butylaminosulphonyl)benzeneboronic acid → 4-(Aminosulphonyl)benzeneboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(tert-Butylaminosulphonyl)benzeneboronic acid | HCID 22107170 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 4-(Aminosulphonyl)benzeneboronic acid | HCID 22391977 | — |
Reaction Steps
A solution of 4-t-butylaminosulfonylbenzene boronic acid (500 mg) in TFA (5 mL) was stirred at r.t. for 15 h. The mixture was diluted with ether and the solid material was filtered to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046217 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-07f470340be640ab8eb15f74be1c9dc0 |
| Source note | uspto-grants-2000_04 |