Butyl iodide → HCID 86587903, compound

HRID 1003673Notes

Reaction equation

HRID 1003673 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#N.I[CH2:11][CH2:12][CH2:13][CH3:14].[C:15]([NH:19][OH:20])([CH3:18])([CH3:17])[CH3:16]>>[CH2:11]([O:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=[N+:19]([C:15]([CH3:18])([CH3:17])[CH3:16])[O-:20])[CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 3

HCID 10962Butyl iodideHCID 119072-HydroxybenzonitrileHCID 98586N-tert-butylhydroxylamine

Product 1

HCID 86587903HCID 86587903, compound

Procedure

The title compound was prepared according to the procedure described in Example 28 using 2-hydroxybenzonitrile, 1-iodobutane and N-tert-butylhydroxylamine. The title compound was isolated in 77.4% overall yield as a viscous oil.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-498f71b895094c2f92d93b4bc2c790a7
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

Loading…