4-Hydroxybenzaldehyde → HCID 74008260, compound

HRID 1003692Notes

Reaction equation

HRID 1003692 reaction equation
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.I[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].[CH3:16][C:17]([N+:20]([O-])=[O:21])([CH3:19])[CH3:18]>>[CH2:11]([O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[N+:20]([C:17]([CH3:19])([CH3:18])[CH3:16])[O-:21])=[CH:4][CH:3]=1)[CH2:12][CH2:13][CH2:14][CH3:15]

Participants

4

Reactant 3

HCID 1264-HydroxybenzaldehydeHCID 116722-Methyl-2-nitropropaneHCID 123351-Iodopentane

Product 1

HCID 74008260HCID 74008260, compound

Procedure

The title compound was prepared according to the procedure described in Example 2 using 4-hydroxybenzaldehyde, 1-iodopentane and 2-methyl-2-nitropropane. The title compound was isolated in 75% overall yield as a solid, m.p. 43.2° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-ac5f07a4bc7049de8208a12f895b324c
Source dataset
uspto-grants-2000_04
Patent number
US06046232

Reaction notes

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