HRID1003744

反应详情

EQUATION

反应方程式

HRID 1003744 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

To 5-(3,4-difluorobenzyl)-4-methoxycarbonyloxazole (0.100 g, 0.393 mmol) in methanol (5 mL) was added 2 mL of 6N HCl, and the solution heated at 80° C. for 2 hours. The reaction mixture was concentrated to yield 0.100 g (88%) of a solid which was used as such for the subsequent step.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated