HuagongsheHuagongshe Chemistry Print Report · For research reference only
Barium Sulfate → 1-(4-(Benzyloxy)phenyl)-4-methylpentan-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Barium Sulfate | HCID 24414 | — |
| Reactant | 1-(4-Benzyloxyphenyl)-4-methyl-pent-1-en-3-one | HCID 471476 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(4-(Benzyloxy)phenyl)-4-methylpentan-3-one | HCID 18798637 | — |
Reaction Steps
Hydrogenation of 50 g (190 mmol) of 1-(4-benzyloxy-phenyl)-4-methyl-pent-1-en-3-one prepared in Example B was effected as described in General Method 3 using 1.08 g 5% Pd over BaSO4 and 1000 mL of THF under hydrogen atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06046355 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-d58ced33f6a04cf7b72a4cc93c1ad377 |
| Source note | uspto-grants-2000_04 |