HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 1-iodo-2,3-dimethoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 3,5-Dimethoxyaniline | HCID 66301 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | 1-iodo-2,3-dimethoxybenzene | HCID 2759363 | — |
Reaction Steps
converting 3,5-dimethoxyaniline into a diazonium salt thereof with using sodium nitrite in acetic acid in the presence of a hydrochloric acid, and reacting the product with potassium iodide to give dimethoxyiodobenzene;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048842 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-e817abf4cc5c4384aa110159b18ed604 |
| Source note | uspto-grants-2000_04 |