Hexane → HCID 18793911, compound

HRID 1003968Notes

Reaction equation

HRID 1003968 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][C:11]([O:13][CH3:14])=[O:12])=[CH:6][CH:5]=1)([CH3:3])[CH3:2].CCCCCC.C(OCC)(=[O:23])C>>[O:23]=[C:10]([C:7]1[CH:8]=[CH:9][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][CH:6]=1)[C:11]([O:13][CH3:14])=[O:12]

Participants

4

Reactant 3

HCID 8058HexaneHCID 8857Ethyl AcetateHCID 12571729HCID 12571729, compound

Product 1

HCID 18793911HCID 18793911, compound

Procedure

Prepared from methyl 4-isopropylphenylacetate by the method described in Example 33a), except that the eluent used was 4:1 hexane:ethyl acetate and the product contained starting material. δH (250 MHz, CDCl3), 1.28 (6H, d, J 6.87), 2.99 (1H, heptet), 3.98 (3H, s), 7.37 (2H, d, J 8.25), 7.95 (2H, d, J 8.33).

Sources & evidence

ORD record
ord-5bb6a85115794094a0e73658a8bc31ca
Source dataset
uspto-grants-2000_04
Patent number
US06048852

Reaction notes

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