Ammonia → HCID 18470624, compound

Participants

Reaction Steps

The subtitle compound was prepared from 2-cyano-3-cyclopentyloxy-4,5-dimethoxynitrobenzene following the procedure described in Example 10(f) and was obtained as a cream coloured solid (66%). Rf 0.79 (dichloromethane:methanol:0.880 aqueous ammonia, 92:7:1, v/v). 1H-NMR (CDCl3): δ=1.57 (2H, m), 1.70 (2H, m), 1.90 (4H, m), 3.68 (3H, s), 3.82 (3H, s), 5.10 (1H, m), 5.98 (1H, s).

Provenance & Evidence