Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | HCID 178487038 | HCID 178487038 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18794229 | HCID 18794229 | — |
Reaction Steps
To a solution of 10-methoxyharmalan in anhydrous ether is added phenyl isocyanate. The mixture is stirred for 1 h 30 and then heated at 45° C. for 30 min. The 1-methylene-2-(N-plienyl)carbamoyl-6-methoxy-1,2,3,4-tetrahydro-β-carboline is recovered by filtration and then washed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06048868 |
|---|
| Source dataset | uspto-grants-2000_04 |
|---|
| ORD ID | ord-a370981202824951af8000935864fe8d |
|---|
| Source note | uspto-grants-2000_04 |
|---|
