HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86755305, compound → HCID 18794426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86755305 | HCID 86755305 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18794426 | HCID 18794426 | — |
Reaction Steps
The compound obtained in Example 6 after Step F is used as substrate, which is treated with a stream of hydrogen in the presence of 10% Pd/C in methanol for 24 hours. Filtration, at the end of the reaction, followed by chromatography over silica gel enables the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048875 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-aae66f96e262421eb610ab7439dfc200 |
| Source note | uspto-grants-2000_04 |