HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20691580, compound → HCID 54334902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20691580 | HCID 20691580 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54334902 | HCID 54334902 | — |
Reaction Steps
A mixture of 13-3 (8.5 g, 28 mmol), 10% Pd/C (1.7 g), and ethanol (140 mL) was stirred under a hydrogen atmosphere for 20 h. The reaction mixture was then filtered through a celite pad and concentrated to give 13-4 as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048861 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-90776d1de0754641a66b4681d52ba8c8 |
| Source note | uspto-grants-2000_04 |