HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20691579, compound → HCID 54211117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20691579 | HCID 20691579 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54211117 | HCID 54211117 | — |
Reaction Steps
To a stirred suspension of 10% palladium on carbon (600 mg) in ethanol (25 mL) was added a solution of 7-[1,8]naphthyridin-2-yl-heptanoic acid methyl ester 29-3 (3.6 g) in ethanol (75 mL) and the mixture was subjected to an atmosphere of hydrogen for 18 hours. The reaction mixture was filtered through Celite and concentrated at reduced pressure to give 29-4 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048861 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-84995f77de4141688d7736368b1f42fb |
| Source note | uspto-grants-2000_04 |