HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2,6-Di-tert-butyl-4-(methoxymethyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Butylated hydroxymethylphenol | HCID 6929 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Product | 2,6-Di-tert-butyl-4-(methoxymethyl)phenol | HCID 6911 | 94% |
Reaction Steps
A solution of 4-hydroxymethyl-2,6-di-t-butylphenol (0.5 g) in methanol (10 mL) containing 1 drop of concentrated hydrochloric acid was stirred at ambient temperature for 1 hour. Evaporation of the solvent gave the title compound, 0.5 g, 94% yield as a white crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06048995 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-113efb57cef44a829e4e591636f562cf |
| Source note | uspto-grants-2000_04 |