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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1004513Generated: October 28, 2026

HCID 70181726, compound → HCID 18794088, compound

https://huagongshe.com/reaction/1004513

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70181726HCID 70181726—
SolventAcetic AcidHCID 176—
SolventHydrochloric AcidHCID 313—
ProductHCID 18794088HCID 18794088—

Reaction Conditions

Temperature50 °C

Reaction Steps

The compound (500 mg) obtained in the above (2) is dissolved in a mixture of 1N hydrochloric acid (5 ml) and acetic acid (5 ml), and the mixture is stirred at 50° C. for 8 hours. The reaction mixture is concentrated under reduced pressure, and the residue is dried to give the title compound (388 mg) as a brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06048854
Source datasetuspto-grants-2000_04
ORD IDord-d8a5353539d145f88b018a2eb39b7e5c
Source noteuspto-grants-2000_04