HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18793167, compound → HCID 18793137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18793167 | HCID 18793167 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 18793137 | HCID 18793137 | 69.5% |
Reaction Steps
A mixture of 3-[m-(benzyloxy)phenoxy]-propionitrile (203 g, 0.80 mol) in 2-propanol is hydrogenated over Raney nickel catalyst (50 g). The catalyst is filtered, and the filtrate is evaporated. Distillation of the residue under high vacuum gives 143 g (69%) of product, bp 190° C. (0.15 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06051605 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-4d20e1b8beca4094a69940d28027c5c2 |
| Source note | uspto-grants-2000_04 |